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Francesco Polizzi
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Let $k$ be an algebraically closed field, ad take $X=\mathbb{P}^2_k$, $U=\mathbb{A}^2_k$.

Then $X$ and $U$ are not homeomorphic, since $U$ contains two disjoint, Zariski-closed, irreducible subsets made of more than one point (think of two parallel lines), but this is not possible in $X$ because of Bézout theorem.

Francesco Polizzi
  • 66.3k
  • 5
  • 180
  • 283